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details VSA-200

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details: ES-XUV

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VSA-200 listing

VSA-200

VSA-200_thumb
In-vacuum selection of optical slits.

Product Details

ES-SXR listing

ES-SXR

High-resolution VLS soft x-ray / EUV flat-field spectrograph.

Resolving power up to ~ 2,000 over a wavelength range ~ 0.6 – 50 nm
or ~ 0.6 – 200 nm, depending on grating complement.

Effective reflection graze angle ~ 2.00 degrees.

Product Details

CAL-32 ANODE LIBRARY listing

CAL-32

Anode_thumbAnodes for electron-beam Manson ultrasoft x-ray light sources.

Product Details

ES-XUV listing

ES-XUV

Ultra-high resolution VLS flat-field spectrograph.

Resolving power up to ~ 20,000 over a wavelength range ~ 1.7 – 30 nm.

Effective reflection graze angle ~ 4.75 degrees.

Product Details

TEFLAT/BLACKFLAT listing

TEFLAT/BLACKFLAT

gaskets_thumbClean & reusable vacuum gaskets

Product Details

SNR-SXR listing

SNR-SXR_thumbSNR-SXR

High-throughput soft x-ray stationary-slit monochromator.

Resolving power ~ 100 over a scanning range ~ 0.6 nm – 10 nm.

Effective reflection graze angle ~ 2.25 degrees.

Product Details

On-site Testing/Optimization listing

Onsite-Testing/Optimization

Expedite “first-light” through the spectrometer in the end-to-end configuration, instruct user on operation and provide advice for system improvement.

On-site fine tuning of the user’s source and detector interfaces to optimize performance (spectral resolution, throughput, etc.)

Perform absolute wavelength calibration of experimentally-obtained spectra.

More Information

Application/Feasibility Analysis listing

Application/Feasibility Analysis

Technical study / written report of custom applications.

More Information

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VSA-200 listing

VSA-200

VSA-200_thumb
In-vacuum selection of optical slits.

Product Details

CAL-32 ANODE LIBRARY listing

CAL-32

Anode_thumbAnodes for electron-beam Manson ultrasoft x-ray light sources.

Product Details

TEFLAT/BLACKFLAT listing

TEFLAT/BLACKFLAT

gaskets_thumbClean & reusable vacuum gaskets

Product Details

Application/Feasibility Analysis listing

Application/Feasibility Analysis

Technical study / written report of custom applications.

More Information

HardwareLeft

VSA-200

VSA-200_thumb
In-vacuum selection of optical slits.

Product Details

CAL-32

Anode_thumbAnodes for electron-beam Manson ultrasoft x-ray light sources.

Product Details

TEFLAT/BLACKFLAT

gaskets_thumbClean & reusable vacuum gaskets

Product Details

ServicesLeft

Application/Feasibility Analysis

Technical study / written report of custom applications.

More Information

Staff

Michael Charles Hettrick


hettrick_thumbCurriculum Vitae

More Information

ES-SXL

Download product pdf


• Erect Field: Small Flat Detection Surface
• Grazing Incidence: Soft X-Ray / EUV / FUV
• VLS: High Spectral Resolution
• Fixed Optics: Robust Stability
• Astigmatic: High Throughput, Compact
• Monochromator Conversion (optional)


ES-SXR Specifications

Mounting
Hettrick, VLS plane grating

Angle-of-Incidence (α)
87.25° (gratings A/B/C/D)
88.75° (SA/SB/SC/SD)
88.00° (focusing mirror)

Replica Grating Format
Gold surface, 62 x 15 mm

Mirror Format
Gold surface, 50 or 100 mm

Vacuum Chamber
9″ X 6″ X 5.5″, plus legs
[Weld-free electroless nickel plated 6061 aluminum]

Vacuum Compatibility
10-8 torr

User ports
TEFLAT/BLACKFLAT gasket-sealed knife-edge flanges – ICF63 (3), ICF114 (1)

Weight
12kg

Source – focal plane
1.75 meters

Meridional Aperture
3.8 mrad (gratings A/B/C/D)
1.75 mrad (SA/SB/SC/SD)

Sagittal Aperture
15 mrad (astigmatic)

curriculum left

Personal


Birthdate: July 29, 1958.
Birthplace: New Britain, Connecticut, U.S.A.

Doctoral Thesis

Selected Journal Publications (28)

More Information

U.S. Letters Patents (4)

More Information

VSA-200 Left

Download product pdf

Slits are required for use under vacuum in spectrometers, imaging systems and interferometers operating at far UV, extreme UV and soft X-ray photon energies.

Model VSA-200 vacuum slit assemblies are used in all Hettrick Scientific spectrometers, and are now available for separate purchase.

ES-XUV details left

Download product pdf


• Erect Field: Small Flat Detection Surface
• Grazing Incidence: XUV
• VLS: Ultra-High Spectral Resolution
• Fixed Optics: Robust Stability
• Astigmatic: High Throughput, Compact
• Monochromator Conversion (optional)


ES-XUV Specifications

Mounting
Hettrick, VLS plane grating

Angle-of-Incidence (α)
87.75°(gratings SX/SA/SB)
85.25°(focusing mirror)

Master Grating Format
Gold surface, 62 x 15 mm

Mirror Format
Gold surface, 50 mm

Vacuum Chamber
9″ X 6″ X 5.5″, plus legs
[Weld-free electroless nickel plated 6061 aluminum]

Vacuum Compatibility
10-8 torr

User ports
TEFLAT/BLACKFLAT™ gasket-sealed knife-edge flanges – ICF070 (3), ICF114 (1)

Weight
12kg

Source – focal plane
5.6 meters

Meridional Aperture
1 mrad

Sagittal Aperture
10 mrad

SNR-SXR

Download product pdf

U.S. Patent 5,274,435

  • Self-Focusing Concave Grating
    – High Throughput
  • Grazing Incidence: Soft X-Ray Use
  • Stationary Slits
  • Fixed Beam Directions
  • Fixed Numerical Aperture
  • Broadband Tunability

Specifications

Mounting
Hettrick, U.S. Patent 5,274,435; Spherical Grating
Angular Deviation
4.5°(Fixed). Nominal graze angle of 2.25°
Grating Stage Format
Gold Surface;
Active Circular Aperture 100 mm
Grating Groove Density
750 g/mm
Wavelength Range
10~100 Angstroms (m=1); approx. 6~50 Angstroms (m=2), depending on source intensity
Fractional Dispersive Resolution
0.167/mm (at Source and Exit Slit)
Optical Aberration (image tilt)
Δλ/λ < 0.010 at 6 mrad Sagittal Aperture, 10~50 Angstroms (m=1)
Meridonial Aperture
12.5 mrad, on Rowland Circle
Sagittal Aperture
0~30 mrad, astigmatic (Φ)
Exit Slit Width (Vacuum Selectable)
200 µm at 0.2°
100 µm at 0.2° (10-13 Å)
100 µm at 0.7° (13-20 Å)
100 µm at 1.2° (20-28 Å)
100 µm at 1.7° (28-37 Å)
100 µm at 2.2° (> 37 Å)
Exit Slit Length
20 mm
External Drive
Single Micro-Stepped Motor with Compumotor ZETA6104-57-83 Indexer/Drive w/RS232C Interface Port
Vacuum Chamber
Weld-Free 6061 Aluminum, Electroless Nickel Plated; TEFLAT/BLACKFLAT Sealed Knife-edge Ports
Entrance and Exit Ports
4.5″ Conflat Flange (ICF114)
User Ports
Three Ports Accept 2.75″ Conflat Flange (ICF070)
Length
0.63 meters (Slit-Slit)
Aperture Center
Stationary

Construction

Model SNR-SXR-0.6 is a high aperture (Φ = 12.5 mrad), single-element soft x-ray Monochromator. The grating has a 100 mm circular aperture with grooves extending to the edge. The distance from (slitless) source to exit slit is 628 mm. The fixed angular deviation of 4.5 degrees and gold coated grating provide efficient reflection to wavelengths as short as λmin = 10 Angstroms in first order and to approximately 6 Angstroms in second order. The spectral resolution is determined by the sagittal aperture which may be set by knife-edges at the entrance port of exit slit, over the range of approximately 0 to 30 mrad. A typical setting of 3 mrad (illuminating 2 mm at the exit slit) provides a fractional spectral resolution of 1/160 at 23 Å, 1/68 at 50 Å, and 1/33 at 100 Å. However, the long wavelength performance is improved considerably by employing an exit slit mask containing 6 slits (100 µm wide) at different angles, to match the image tilt over different regions in scanned wavelength. Using the appropriate slit, the resolution is approximately 1/100 over 10~50 Å using a 6 mrad sagittal aperture.

An externally mounted micro-stepping motor with Compumotor indexer provides rotational control of the grating scan under vacuum by means of a shaft feedthrough. The slits are also selectable under vacuum using a micrometer shaft feedthrough. Both the grating chamber and the slit chambers are electroless-nickel plated aluminum and are machined square relative to the grating surface and slit mask, enabling alignment by mechanical indication from the chamber exteriors.

The photograph shows a custom system including model SNR-SXR-0.6 and associated optional equipment (not included with base instrument) such as a Manson model 2 soft x-ray source and compact chamber, pumps, gages, mounting table and brackets, CCD, filter assembly, vacuum-selectable aperture and microscope visible alignment system, for calibrating x-ray transmission gratings in the 5-114 Å region.

snr-sxr-fig3

CAL-32

Download product pdf

These anode cap sets are designed to be used with the Manson electron impact sources1, models 2 and 5. As enumerated in the table, the anode library provides a multitude of characteristic lines from K, L and M-shell transitions, as well as Bremsstrahlung continua. The ability to select spectral lines at closely spaced soft x-ray photon energies allows the calibration of spectral features such as filter absorption edges, multilayer (Bragg) interference reflectance peaks and grating efficiency variations (see Fig. 2) without resorting to the use of a synchrotron radiation facility.

The same anode set fits both model 2 and model 5 Manson sources. As specified for each material in the table, the anode caps are constructed of either a) the metal itself, or b) a base of 303 stainless steel with the impact material affixed to the top using low-outgassing silver conductive epoxy. Each anode cap is vented and, following initial break-in, is compatible with vacuum into the 10-8 mbar range. With the exception of Be, all anode caps are reusable indefinitely by nylon pad cleaning of the anode surface after extended use.

Fig. 1 shows the spectrum produced by one typical anode material (zinc), consisting of several useable characteristic L-shell lines, plus an underlying continuum for the atomic number Z=30. As the Bremsstrahlung strength is highly dependent upon Z, the strongest continuum is obtained using tantalum (Z=73) or tungsten (Z=74). Anode set model CAL-32 comprises the following materials: Be(4), B, C, Sapphire, Mg, Al, Si, Sc, Ti, V, Cr, Mn, Fe, SS303, Co, Ni, Cu, Zn, Ge, Y, Zr, Nb, Mo, Ru,Pd, Ag, Sn, Ta and W); refer to the characteristic emission line table for the available photon energies.

As an option, enhanced cooling of the operating anodes is available, using forced-air fans combined with a copper-block finned radiator. This is found to improve the positional stability of the emission region of the Manson source and stabilize its output intensity through reduced hydrocarbon contamination.

cal-32-fig1

Fig. 1. Spectrum of characteristic lines and Bremsstrahlung continuum from a zinc anode in the Manson model 2 source, using Hettrick SXR-II spectrometer and a CCD detector to record the spectrum.

cal-32-fig2
Fig. 2. Absolute efficiency measurements of a free-standing transmission grating, using numerous characteristic lines from CAL-32 anode library and Hettrick SXR-II monochromator.

1 Manson electron impact sources are manufactured and sold by Austin Instruments, Inc.
website: www.austinst.com
email: austinst@tiac.net
tel: 800-818-7403.

Ultimate Posts

Download product pdf

TEFLAT™/BLACKFLAT™ gaskets provide many advantages when compared to conventional sealing materials for knife-edge flanges:

• Require much less force than copper, significantly reducing assembly time (and saving knuckles!).
• May be used with aluminum (or stainless steel) flanges and ports.
• Unlike copper gaskets, Teflon® gaskets are reusable, if not removed from flange and kept clean (number of re-uses may vary).
• Unlike copper gaskets, Teflon® gaskets do not tarnish with exposure to air.
• Unlike copper gaskets or o-rings, Teflon® does not react with most chemicals.
• Avoids the use of grease often necessary to keep thin section o-rings registered in place during assembly, particularly for a vertical flange orientation.
• Minimizes contamination of vacuum systems, particularly important for coating applications, high purity analyses and ultra-high vacuum applications.
• Unlike thin section o-rings, rigid Teflon® gaskets self-locate against the flange lip to provide a clear confirmation of a correct seal, preventing leaks and extruded o-rings.
• Less expensive than rectangular section o-rings.

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