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details VSA-200

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details ES-XUV

details: ES-XUV

CAL-32

CAL-32 Custom Anode Library

details SNR-SXR

details: SNR-SXR

details TEFLAT/BLACKFLAT

details: TEFLAT-BLACKFLAT

Asides

Application/Feasibility Analyses main

Application/Feasibility Analyses

Prior to the purchase of a spectrometer or other hardware, the customer is often in need of a proper study on the feasibility of applying such an optical system to obtain the desired experimental result. As the inventor of all Hettrick Scientific spectrographs and monochromators and an expert in the field of soft x-ray and extreme UV optics, Dr. Michael C. Hettrick performs such technical analyses upon request for a fixed quoted fee. The study typically culminates in a written report, summarizing the salient findings and providing the scientist/engineer with a set of practical options for achieving the desired result in a timely and economical manner.

As a paid professional consultant, Dr. Hettrick will provide an unbiased analysis. The customer may instruct that the study either be restricted to a comparison of the detailed trade-offs and optimization in applying the various instruments available for sale by Hettrick Scientific, or be a more general technical analysis not geared towards expediting a sale of our products.

On-site Testing/Optimization main

On-site Testing/Optimization

These services are provided at an hourly on-site rate.

Recent Research

RECENT RESEARCH

“Divergent groove gratings: wavelength scanning in fixed geometry spectrometers,” M.C. Hettrick, Opt. Express vol. 24, 26646-26666 (2016).

“A single-element plane grating monochromator,” M.C. Hettrick, Photonics, vol. 3(1), no. 3:1-44 (2016).

Supplementary material (Figure 3 animation) for “A single-element plane grating monochromator”
– download animation (29M)

“Corrections to ‘A Single-Element Plane Grating Monochromator’,” M.C. Hettrick, www.hettrickscientific.com (2016).

curriculum vitae left

Personal


Birthdate: July 29, 1958.
Birthplace: New Britain, Connecticut, U.S.A.

Doctoral Thesis

Selected Journal Publications (28)

More Information

U.S. Letters Patents (4)

More Information

Curriculum vitae main

Education and Professional Experience


1976-1980
Undergraduate student, Rensselaer Polytechnic Institute (Troy, NY); United Technologies academic scholarship; research assistant in radio astronomy and theoretical astrophysics; member Society of Physics Students and American Astronomical Society; volunteer physics tutor.  Graduated magna cum laude, B.S. in Physics, minors in Mathematics and Astronomy.

1980-1981
Graduate student, Dept. Astronomy, University of California at Berkeley, under a graduate fellowship; teaching assistant.

1981-1987
Research Scientist, University of California at Berkeley: Space Sciences Laboratory, Physics Department and Lawrence Berkeley Laboratory; invented several satellite and laboratory optical systems, including the grazing incidence spectrometers flown aboard the Extreme Ultraviolet Explorer (EUVE) and the XMM-Newton soft x-ray observatory.

1987- present
Founder, owner and sole operator of Hettrick Scientific.  Designed and manufactured grazing incidence spectrometers and optics sold to universities, national laboratories and companies worldwide for physics research.  Twice (1988, 1992) received the “R&D 100 award” for developing one of the 100 “most significant technical products” of the year.

1996
Doctoral thesis, “Optical Design and Experimental Development of Grazing Incidence Fixed Slit Spectrometers for High Resolution Plasma Diagnostics”, The Graduate University for Advanced Studies, Department of Fusion Science, Gifu, Japan, 1996.

Doctoral Thesis

Michael Charles Hettrick listing

Michael Charles Hettrick


hettrick_thumbCurriculum Vitae

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academic-journal listing

Selected Journal Publications


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post ES-SXR details left

Download product pdf


• Erect Field: Small Flat Detection Surface
• Grazing Incidence: Soft X-Ray / EUV / FUV
• VLS: High Spectral Resolution
• Fixed Optics: Robust Stability
• Astigmatic: High Throughput, Compact
• Monochromator Conversion (optional)


ES-SXR Specifications

Mounting
Hettrick, VLS plane grating

Angle-of-Incidence (α)
87.25° (gratings A/B/C/D)
88.75° (SA/SB/SC/SD)
88.00° (focusing mirror)

Replica Grating Format
Gold surface, 62 x 15 mm

Mirror Format
Gold surface, 50 or 100 mm

Vacuum Chamber
9″ X 6″ X 5.5″, plus legs
[Weld-free electroless nickel plated 6061 aluminum]

Vacuum Compatibility
10-8 torr

User ports
TEFLAT/BLACKFLAT gasket-sealed knife-edge flanges – ICF63 (3), ICF114 (1)

Weight
12kg

Source – focal plane
1.75 meters

Meridional Aperture
3.8 mrad (gratings A/B/C/D)
1.75 mrad (SA/SB/SC/SD)

Sagittal Aperture
15 mrad (astigmatic)

Quality Control Supervisor listing

Quality Control Supervisor


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ES-SXR details main

Opto-Mechanical Design

A grazing incidence varied line-space (VLS) diffraction grating provides a normal incidence spectrum, allowing efficient use of CCD and other electronic detectors. The Edge Spectrograph is an astigmatic, fixed-optic design, with model ES-SXR providing a resolving power up to ~ 2,000. Initially applied to analyzing the K-edges of Silicon and Oxygen for CCD characterization and those of Aluminum and Oxygen for thin-film filter calibration, the design has also proven ideal for characterization of LPP, HHG and Z-pinch light sources. There are no feedthrough adjustments of the optics, resulting in a simple, low-cost design. Each grating is mounted to a dedicated vacuum flange which is exchanged at atmosphere to select the desired spectral region. Fine-tuning of the spectral focus is achieved by the user adjusting his point source position.

Alternatively, an optional entrance slit assembly provides a micrometer feedthrough positioning adjustment of the slits, for use with a spatially extended source. Four manually-adjustable honed knife-edges at the entrance port of the optics chamber define the illuminated aperture, and one knife-edge is placed at the position of minimum confusion above the focusing mirror to reduce stray light. The aluminum optics chamber is supplied with mounting legs which can be bolted directly to an inch-spacing threaded hole (1/4-20) user-supplied breadboard. The user also provides the light source and detector along with their connecting nipples to the optics chamber, and vacuum pumps/gages.

The spectrograph includes 4 replica gratings (SA/SB/SC/SD or A/B/C/D), each mounted on a dedicated ICF114 knife-edge flange with engraved nameplate and gasket-sealed storage cylinder. Absolute efficiency calibrations of sample gratings SA, SB and SC are given in Fig. 2.

Conversion to a monochromator may be conveniently implemented by the user providing a simple linear translation of the light source along the erect flat-field spectral plane. In this case, the direction of propagation is reversed such that a stationary exit slit is positioned in place of the light source shown on the left side of the optical schematic (Fig. 1). Details of such a conversion depend upon the optical and mechanical characteristics of the user’s light source, and should be discussed with Hettrick Scientific to evaluate its feasibility and ease-of-use for the intended application.
This spectrograph/monochromator workhorse provides access to over two decades in wavelength (6 ~ 2000 Angstroms) covering the soft x-ray, EUV and FUV spectral regions.


Grating Band Specifications

ES-SCR_GratingTable

Fig. 1. Schematic of ES-SXR optical system. The flat-field spectrum is dispersed about the center wavelength (λc) onto a normal incidence detector. In this standard mounting, dispersion is vertical and the optical axes incident and exiting the optics chamber are at sea-level.
Efficiency Calibration
es-sxr-fig1

Fig. 2. Efficiency calibration of individual replica gratings. Angle-of-incidence is 88.75°. Illuminated region within active ru1ed aperture of 15 mm x 62.5 mm is approximately 5 mm along groove lengths by 5-20 mm in ruled width direction, depending upon the wavelength. These results are certified only for these specific serial number gratings and do not constitute a representation or approximation of efficiencies which may be obtained with other individual replicas or at other angles of incidence.

es-sxr-fig2

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VSA-200 listing

VSA-200

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In-vacuum selection of optical slits.

Product Details

CAL-32 ANODE LIBRARY listing

CAL-32

Anode_thumbAnodes for electron-beam Manson ultrasoft x-ray light sources.

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TEFLAT/BLACKFLAT listing

TEFLAT/BLACKFLAT

gaskets_thumbClean & reusable vacuum gaskets

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Application/Feasibility Analysis listing

Application/Feasibility Analysis

Technical study / written report of custom applications.

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HardwareLeft

VSA-200

VSA-200_thumb
In-vacuum selection of optical slits.

Product Details

CAL-32

Anode_thumbAnodes for electron-beam Manson ultrasoft x-ray light sources.

Product Details

TEFLAT/BLACKFLAT

gaskets_thumbClean & reusable vacuum gaskets

Product Details

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Application/Feasibility Analysis

Technical study / written report of custom applications.

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Staff

Michael Charles Hettrick


hettrick_thumbCurriculum Vitae

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ES-SXL

Download product pdf


• Erect Field: Small Flat Detection Surface
• Grazing Incidence: Soft X-Ray / EUV / FUV
• VLS: High Spectral Resolution
• Fixed Optics: Robust Stability
• Astigmatic: High Throughput, Compact
• Monochromator Conversion (optional)


ES-SXR Specifications

Mounting
Hettrick, VLS plane grating

Angle-of-Incidence (α)
87.25° (gratings A/B/C/D)
88.75° (SA/SB/SC/SD)
88.00° (focusing mirror)

Replica Grating Format
Gold surface, 62 x 15 mm

Mirror Format
Gold surface, 50 or 100 mm

Vacuum Chamber
9″ X 6″ X 5.5″, plus legs
[Weld-free electroless nickel plated 6061 aluminum]

Vacuum Compatibility
10-8 torr

User ports
TEFLAT/BLACKFLAT gasket-sealed knife-edge flanges – ICF63 (3), ICF114 (1)

Weight
12kg

Source – focal plane
1.75 meters

Meridional Aperture
3.8 mrad (gratings A/B/C/D)
1.75 mrad (SA/SB/SC/SD)

Sagittal Aperture
15 mrad (astigmatic)

curriculum left

Personal


Birthdate: July 29, 1958.
Birthplace: New Britain, Connecticut, U.S.A.

Doctoral Thesis

Selected Journal Publications (28)

More Information

U.S. Letters Patents (4)

More Information

VSA-200 Left

Download product pdf

Slits are required for use under vacuum in spectrometers, imaging systems and interferometers operating at far UV, extreme UV and soft X-ray photon energies.

Model VSA-200 vacuum slit assemblies are used in all Hettrick Scientific spectrometers, and are now available for separate purchase.

ES-XUV details left

Download product pdf


• Erect Field: Small Flat Detection Surface
• Grazing Incidence: XUV
• VLS: Ultra-High Spectral Resolution
• Fixed Optics: Robust Stability
• Astigmatic: High Throughput, Compact
• Monochromator Conversion (optional)


ES-XUV Specifications

Mounting
Hettrick, VLS plane grating

Angle-of-Incidence (α)
87.75°(gratings SX/SA/SB)
85.25°(focusing mirror)

Master Grating Format
Gold surface, 62 x 15 mm

Mirror Format
Gold surface, 50 mm

Vacuum Chamber
9″ X 6″ X 5.5″, plus legs
[Weld-free electroless nickel plated 6061 aluminum]

Vacuum Compatibility
10-8 torr

User ports
TEFLAT/BLACKFLAT™ gasket-sealed knife-edge flanges – ICF070 (3), ICF114 (1)

Weight
12kg

Source – focal plane
5.6 meters

Meridional Aperture
1 mrad

Sagittal Aperture
10 mrad

SNR-SXR

Download product pdf

U.S. Patent 5,274,435

  • Self-Focusing Concave Grating
    – High Throughput
  • Grazing Incidence: Soft X-Ray Use
  • Stationary Slits
  • Fixed Beam Directions
  • Fixed Numerical Aperture
  • Broadband Tunability

Specifications

Mounting
Hettrick, U.S. Patent 5,274,435; Spherical Grating
Angular Deviation
4.5°(Fixed). Nominal graze angle of 2.25°
Grating Stage Format
Gold Surface;
Active Circular Aperture 100 mm
Grating Groove Density
750 g/mm
Wavelength Range
10~100 Angstroms (m=1); approx. 6~50 Angstroms (m=2), depending on source intensity
Fractional Dispersive Resolution
0.167/mm (at Source and Exit Slit)
Optical Aberration (image tilt)
Δλ/λ < 0.010 at 6 mrad Sagittal Aperture, 10~50 Angstroms (m=1)
Meridonial Aperture
12.5 mrad, on Rowland Circle
Sagittal Aperture
0~30 mrad, astigmatic (Φ)
Exit Slit Width (Vacuum Selectable)
200 µm at 0.2°
100 µm at 0.2° (10-13 Å)
100 µm at 0.7° (13-20 Å)
100 µm at 1.2° (20-28 Å)
100 µm at 1.7° (28-37 Å)
100 µm at 2.2° (> 37 Å)
Exit Slit Length
20 mm
External Drive
Single Micro-Stepped Motor with Compumotor ZETA6104-57-83 Indexer/Drive w/RS232C Interface Port
Vacuum Chamber
Weld-Free 6061 Aluminum, Electroless Nickel Plated; TEFLAT/BLACKFLAT Sealed Knife-edge Ports
Entrance and Exit Ports
4.5″ Conflat Flange (ICF114)
User Ports
Three Ports Accept 2.75″ Conflat Flange (ICF070)
Length
0.63 meters (Slit-Slit)
Aperture Center
Stationary

Construction

Model SNR-SXR-0.6 is a high aperture (Φ = 12.5 mrad), single-element soft x-ray Monochromator. The grating has a 100 mm circular aperture with grooves extending to the edge. The distance from (slitless) source to exit slit is 628 mm. The fixed angular deviation of 4.5 degrees and gold coated grating provide efficient reflection to wavelengths as short as λmin = 10 Angstroms in first order and to approximately 6 Angstroms in second order. The spectral resolution is determined by the sagittal aperture which may be set by knife-edges at the entrance port of exit slit, over the range of approximately 0 to 30 mrad. A typical setting of 3 mrad (illuminating 2 mm at the exit slit) provides a fractional spectral resolution of 1/160 at 23 Å, 1/68 at 50 Å, and 1/33 at 100 Å. However, the long wavelength performance is improved considerably by employing an exit slit mask containing 6 slits (100 µm wide) at different angles, to match the image tilt over different regions in scanned wavelength. Using the appropriate slit, the resolution is approximately 1/100 over 10~50 Å using a 6 mrad sagittal aperture.

An externally mounted micro-stepping motor with Compumotor indexer provides rotational control of the grating scan under vacuum by means of a shaft feedthrough. The slits are also selectable under vacuum using a micrometer shaft feedthrough. Both the grating chamber and the slit chambers are electroless-nickel plated aluminum and are machined square relative to the grating surface and slit mask, enabling alignment by mechanical indication from the chamber exteriors.

The photograph shows a custom system including model SNR-SXR-0.6 and associated optional equipment (not included with base instrument) such as a Manson model 2 soft x-ray source and compact chamber, pumps, gages, mounting table and brackets, CCD, filter assembly, vacuum-selectable aperture and microscope visible alignment system, for calibrating x-ray transmission gratings in the 5-114 Å region.

snr-sxr-fig3

CAL-32

Download product pdf

These anode cap sets are designed to be used with the Manson electron impact sources1, models 2 and 5. As enumerated in the table, the anode library provides a multitude of characteristic lines from K, L and M-shell transitions, as well as Bremsstrahlung continua. The ability to select spectral lines at closely spaced soft x-ray photon energies allows the calibration of spectral features such as filter absorption edges, multilayer (Bragg) interference reflectance peaks and grating efficiency variations (see Fig. 2) without resorting to the use of a synchrotron radiation facility.

The same anode set fits both model 2 and model 5 Manson sources. As specified for each material in the table, the anode caps are constructed of either a) the metal itself, or b) a base of 303 stainless steel with the impact material affixed to the top using low-outgassing silver conductive epoxy. Each anode cap is vented and, following initial break-in, is compatible with vacuum into the 10-8 mbar range. With the exception of Be, all anode caps are reusable indefinitely by nylon pad cleaning of the anode surface after extended use.

Fig. 1 shows the spectrum produced by one typical anode material (zinc), consisting of several useable characteristic L-shell lines, plus an underlying continuum for the atomic number Z=30. As the Bremsstrahlung strength is highly dependent upon Z, the strongest continuum is obtained using tantalum (Z=73) or tungsten (Z=74). Anode set model CAL-32 comprises the following materials: Be(4), B, C, Sapphire, Mg, Al, Si, Sc, Ti, V, Cr, Mn, Fe, SS303, Co, Ni, Cu, Zn, Ge, Y, Zr, Nb, Mo, Ru,Pd, Ag, Sn, Ta and W); refer to the characteristic emission line table for the available photon energies.

As an option, enhanced cooling of the operating anodes is available, using forced-air fans combined with a copper-block finned radiator. This is found to improve the positional stability of the emission region of the Manson source and stabilize its output intensity through reduced hydrocarbon contamination.

cal-32-fig1

Fig. 1. Spectrum of characteristic lines and Bremsstrahlung continuum from a zinc anode in the Manson model 2 source, using Hettrick SXR-II spectrometer and a CCD detector to record the spectrum.

cal-32-fig2
Fig. 2. Absolute efficiency measurements of a free-standing transmission grating, using numerous characteristic lines from CAL-32 anode library and Hettrick SXR-II monochromator.

1 Manson electron impact sources are manufactured and sold by Austin Instruments, Inc.
website: www.austinst.com
email: austinst@tiac.net
tel: 800-818-7403.

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Download product pdf

TEFLAT™/BLACKFLAT™ gaskets provide many advantages when compared to conventional sealing materials for knife-edge flanges:

• Require much less force than copper, significantly reducing assembly time (and saving knuckles!).
• May be used with aluminum (or stainless steel) flanges and ports.
• Unlike copper gaskets, Teflon® gaskets are reusable, if not removed from flange and kept clean (number of re-uses may vary).
• Unlike copper gaskets, Teflon® gaskets do not tarnish with exposure to air.
• Unlike copper gaskets or o-rings, Teflon® does not react with most chemicals.
• Avoids the use of grease often necessary to keep thin section o-rings registered in place during assembly, particularly for a vertical flange orientation.
• Minimizes contamination of vacuum systems, particularly important for coating applications, high purity analyses and ultra-high vacuum applications.
• Unlike thin section o-rings, rigid Teflon® gaskets self-locate against the flange lip to provide a clear confirmation of a correct seal, preventing leaks and extruded o-rings.
• Less expensive than rectangular section o-rings.

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