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ES-SXR

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Publications

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Applications

details VSA-200

Applications

details ES-XUV

details: ES-XUV

CAL-32

CAL-32 Custom Anode Library

details SNR-SXR

details: SNR-SXR

details TEFLAT/BLACKFLAT

details: TEFLAT-BLACKFLAT

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Applications main

Customer applications of Hettrick Scientific spectrographs and monochromators

  • Inertial confinement fusion (ICF) energy diagnostics
  • Characterization of soft x-ray and extreme UV plasma light sources
  • Basic research (e.g. gain-narrowing and coherence length) on soft x-ray/EUV lasers
  • Pre-flight long-beam calibration of astronomical telescope end-to-end payloads (ASTRO-D, AXAF, XMM)
  • Study of QE and charge-transfer in soft x-ray detectors (diodes, MCPs, CCDs and micro-calorimeters)
  • XAFS analysis of oxidized dead layer (O-K edge) in CCDs
  • Thin-film soft x-ray filter transmission measurements
  • Synthetic multilayer mirror reflectance rocking curve measurements
  • Absolute efficiency calibration and physical model parameter fitting of soft x-ray free-standing transmission gratings
  • Radiometric spectral measurement of high-power Z-pinch sources
  • Basic physics on Z-pinch driven soft x-ray hohlraums
  • Planckian kT determination of pulsed-laser driven EUV hohlraums
  • Femtosecond HHG (high harmonic generation) source characterization and spectral selection
  • Nanosecond and picosecond LPP (laser-produced plasma) source applications, including solid and liquid jet targets
  • Trans-uranic element photo-electron surface analysis
  • Measurement of temporal coherence length in soft x-ray interferometry
  • Manson (electron-beam) source spectral filtering of Bremsstrahlung and selection of characteristic emission lines

Quality Control main


Please click on my photo!

Chappy Publications

“Sleep – check … Bark – check … Sleep – check … Eat – check
—— BUSY DAY —— time to rest,” Chappy, Proc. Soc. Retired Canines (2015).

“I’m a Dog ….. I CAN’T ‘SPEAK’ ….. Just Give Me the Snack !” Chappy, Invited Lecture – Soc. Cognitive Res. (2014).

“How to Avoid Punishment by Volunteering it with a Guilty Face,” Chappy, J. Human Psychol. (2013).

“I am as Big as my Bark ……… or ….…. How I Learned to Stop Worrying and Love Provoking Shiba Inu’s,” Chappy, Failed Breeds of Artif. Selection (2012).

“To Understand a Cat, First Think of a Dog — then Subtract Loyalty and Trust,” Chappy, Cats ‘r Jerks – Vol. III (2011).

“The Best Hiding Places to Escape Taking a Bath,” Chappy, Diary entry (2010).

“The 101 Smells of Nogawa Park,” Chappy, Thesis (2009).

“This is MY Cave,” Chappy, Canine Homestead Act (2008).

“Men in White Touch Me in Inappropriate Places …….. get me OUT of here !” Chappy, Annals of the Coalition for Lonely Veterinarians (2007).

“The Health Benefits of Eating Shrimp Tails,” Chappy, Health and Nutr. Sci. (2006).

“Quickies with the Cute Young Bitch Next Door,” Chappy, J. Anim. Reprod. (2005).

“The Principle of Maximizing the Path-Length of a Walk through the Park,” Chappy, priv. communication – Fermat’s Dog (2004).

“Dinner Guests are Suckers for Free Food,” Chappy, J. Human Psychol. (2003).

“My Tongue is Cleaner than a Human’s …. are you SURE ?!” Chappy, Int. Symposium on Shameless Hygienics (2002).

“If it Falls on the Floor, It’s Mine,” Chappy, Common Law Review – Chapter 1 (2001).

Supplementary Material


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Patents main

Patents

Optical System For High Resolution Spectrometer/Monochromator
Patent #:
4776696

Aplanatic and Quasi-Aplanatic Diffraction Gratings
Patent #:
4798446

Varied Space Diffraction Grating and In-Focus Monochromator
Patent #:
4991934

Grating Monochromators and Spectrometers Based on Surface Normal Rotation
Patent #:
5274435

Academic Journal Publications main

“Divergent groove gratings: wavelength scanning in fixed geometry spectrometers,” Hettrick, Opt. Express vol. 24, 26646-26666 (2016).

“Corrections to ‘A Single-Element Plane Grating Monochromator’,” Hettrick, www.hettrickscientific.com (2016).

“A single-element plane grating monochromator,” Hettrick, Photonics vol. 3(1), no. 3:1-44 (2016).

“Refined self-calibration of silicon photodiode efficiencies using a compact soft x-ray apparatus,” Hettrick et al., preprint (2011).

“Characteristics and scaling of tungsten-wire-array z-pinch implosion dynamics at 20 MA,” Cuneo et al., Phys. Rev. E 71, 046406 (2005).

“Profiled bar transmission gratings: soft x-ray calibration of new Kirchoff solutions,” Hettrick et al., Appl. Opt. vol. 43, pp. 3772-3796 (2004).

“Profiled bar transmission gratings: soft-x-ray calibration of new Kirchoff solutions—erratum,” Appl. Opt., vol. 43, p. 4785 (2004).

“Surface normal rotation: a new technique for grazing-incidence monochromators,” Hettrick, Appl. Opt. vol. 31, pp. 7174-7178 (1992).

“In-focus monochromator: theory and experiment of a new grazing incidence mounting,” Hettrick, Appl. Opt. vol. 29, pp. 4531-4535 (1990).

“High resolution gratings for the soft x-ray,” Hettrick, Nucl. Instrum. Meth. vol. A266, pp. 404-413 (1988).

“Resolving power of 35,000 (5 mA) in the extreme ultraviolet employing a grazing incidence spectrometer,” Hettrick et al., Appl. Opt. vol. 27, pp. 200-202 (1988).

“Maximum – a scanning photoelectron microscope at Alladin,” Cerrina et al., Nucl. Instrum. Meth. vol. A266, pp. 303-307 (1988).

“A beam line for layered synthetic microstructure studies,” Boudry et al., Nucl. Instrum. Meth. vol. A266, pp. 351-355 (1988).

“Laboratory astrophysics experiments in x-ray transfer physics relevant to cosmic accretion-powered sources,” Kahn et al., J. de Physique vol. 49 (colloque C1), 67 (1988).

“High resolution krypton M4.5 x-ray emission spectra,” Perera et al., X-Ray and Inner-Shell Processes Vol. 1, J. Phys. Colloques vol. 48 (1987).

“Stigmatic high throughput monochromator for soft x-rays,” Hettrick et al., Appl. Opt. vol. 25, pp. 4228-4231 (1986).

“Aplanatic grazing incidence diffraction grating: a new optical element,” Hettrick, Appl. Opt. vol. 25, pp. 3269-3282 (1986).

“Varied line-space gratings: past, present and future,” Hettrick, Proc. Soc. Photo-Opt. Instrum. Eng. vol. 560, pp. 96-108 (1986).

“A reflection grating spectrometer for the x-ray multi-mirror (XMM) space observatory – design and calculated performance, “Hettrick et al., Proc. Soc. Photo-Opt. Instrum. Eng. vol. 597, pp. 291-300 (1986).

“Grazing incidence reflection coefficients of rhodium, osmium, platinum and gold from 50 to 300 A,” Hettrick et al., Appl. Opt. vol. 24, pp. 3682-3685 (1985).

“Grazing incidence echelle spectrometers using varied line-space gratings,” Hettrick, Appl. Opt. vol. 24, pp. 1251-1255 (1985).

“Molybdenum-silicon multilayer mirrors for the extreme ultraviolet,” Barbee et al., Appl. Opt. vol. 24, pp. 883-886 (1985).

“Extreme ultraviolet explorer spectrometer,” Hettrick et al., Appl. Opt. vol. 25, pp. 1737-1756 (1985).

“Extreme UV measurements of a varied line-space Hitachi reflection grating: efficiency and scattering,” Edelstein et al., Appl. Opt. vol. 23, pp. 3267-3270 (1984).

“Proposed design class of grazing incidence echelle spectrometers: critical analysis and reevaluation,” Hettrick et al., Appl. Opt. vol. 23, pp. 4058-4066 (1984).

“Grazing incidence telescopes: a new class for soft x-ray and EUV spectroscopy,” Hettrick et al., Appl. Opt. vol. 23, pp. 3732-3735 (1984).

“Grazing incidence telescopes: a new class for soft x-ray and EUV spectroscopy; addendum,” Hettrick et. al., vol. 24, p. 929 (1985).

“Interference methods in the testing and fabrication of new-design grazing incidence gratings,” Hettrick et al., Proc. Soc. Photo-Opt. Instrum. Eng., vol. 503, pp. 106-113 (1984)

“Aberrations of varied line-space grazing incidence gratings in converging light beams,” Hettrick, Appl. Opt. vol. 23, pp. 3221-3235 (1984).

“Variable line-space gratings: new designs for use in grazing incidence spectrometers,” Hettrick et al., Appl. Opt. vol. 22, pp. 3921-3924 (1983).

“Maximizing the quantum efficiency of microchannel-plate detectors: the collection of photoelectrons from the interchannel web using an electric field,” Taylor et al., Rev. Sci. Instrum. Vol. 54, pp. 171-176 (1983).

“Velocity structure in the Canis Major R1 molecular clouds,” Machnik et al., ” Astrophys. J. vol. 242, pp. 121-131 (1980).

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VSA-200 listing

VSA-200

VSA-200_thumb
In-vacuum selection of optical slits.

Product Details

CAL-32 ANODE LIBRARY listing

CAL-32

Anode_thumbAnodes for electron-beam Manson ultrasoft x-ray light sources.

Product Details

TEFLAT/BLACKFLAT listing

TEFLAT/BLACKFLAT

gaskets_thumbClean & reusable vacuum gaskets

Product Details

Application/Feasibility Analysis listing

Application/Feasibility Analysis

Technical study / written report of custom applications.

More Information

HardwareLeft

VSA-200

VSA-200_thumb
In-vacuum selection of optical slits.

Product Details

CAL-32

Anode_thumbAnodes for electron-beam Manson ultrasoft x-ray light sources.

Product Details

TEFLAT/BLACKFLAT

gaskets_thumbClean & reusable vacuum gaskets

Product Details

ServicesLeft

Application/Feasibility Analysis

Technical study / written report of custom applications.

More Information

Staff

Michael Charles Hettrick


hettrick_thumbCurriculum Vitae

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ES-SXL

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• Erect Field: Small Flat Detection Surface
• Grazing Incidence: Soft X-Ray / EUV / FUV
• VLS: High Spectral Resolution
• Fixed Optics: Robust Stability
• Astigmatic: High Throughput, Compact
• Monochromator Conversion (optional)


ES-SXR Specifications

Mounting
Hettrick, VLS plane grating

Angle-of-Incidence (α)
87.25° (gratings A/B/C/D)
88.75° (SA/SB/SC/SD)
88.00° (focusing mirror)

Replica Grating Format
Gold surface, 62 x 15 mm

Mirror Format
Gold surface, 50 or 100 mm

Vacuum Chamber
9″ X 6″ X 5.5″, plus legs
[Weld-free electroless nickel plated 6061 aluminum]

Vacuum Compatibility
10-8 torr

User ports
TEFLAT/BLACKFLAT gasket-sealed knife-edge flanges – ICF63 (3), ICF114 (1)

Weight
12kg

Source – focal plane
1.75 meters

Meridional Aperture
3.8 mrad (gratings A/B/C/D)
1.75 mrad (SA/SB/SC/SD)

Sagittal Aperture
15 mrad (astigmatic)

curriculum left

Personal


Birthdate: July 29, 1958.
Birthplace: New Britain, Connecticut, U.S.A.

Doctoral Thesis

Selected Journal Publications (28)

More Information

U.S. Letters Patents (4)

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VSA-200 Left

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Slits are required for use under vacuum in spectrometers, imaging systems and interferometers operating at far UV, extreme UV and soft X-ray photon energies.

Model VSA-200 vacuum slit assemblies are used in all Hettrick Scientific spectrometers, and are now available for separate purchase.

ES-XUV details left

Download product pdf


• Erect Field: Small Flat Detection Surface
• Grazing Incidence: XUV
• VLS: Ultra-High Spectral Resolution
• Fixed Optics: Robust Stability
• Astigmatic: High Throughput, Compact
• Monochromator Conversion (optional)


ES-XUV Specifications

Mounting
Hettrick, VLS plane grating

Angle-of-Incidence (α)
87.75°(gratings SX/SA/SB)
85.25°(focusing mirror)

Master Grating Format
Gold surface, 62 x 15 mm

Mirror Format
Gold surface, 50 mm

Vacuum Chamber
9″ X 6″ X 5.5″, plus legs
[Weld-free electroless nickel plated 6061 aluminum]

Vacuum Compatibility
10-8 torr

User ports
TEFLAT/BLACKFLAT™ gasket-sealed knife-edge flanges – ICF070 (3), ICF114 (1)

Weight
12kg

Source – focal plane
5.6 meters

Meridional Aperture
1 mrad

Sagittal Aperture
10 mrad

SNR-SXR

Download product pdf

U.S. Patent 5,274,435

  • Self-Focusing Concave Grating
    – High Throughput
  • Grazing Incidence: Soft X-Ray Use
  • Stationary Slits
  • Fixed Beam Directions
  • Fixed Numerical Aperture
  • Broadband Tunability

Specifications

Mounting
Hettrick, U.S. Patent 5,274,435; Spherical Grating
Angular Deviation
4.5°(Fixed). Nominal graze angle of 2.25°
Grating Stage Format
Gold Surface;
Active Circular Aperture 100 mm
Grating Groove Density
750 g/mm
Wavelength Range
10~100 Angstroms (m=1); approx. 6~50 Angstroms (m=2), depending on source intensity
Fractional Dispersive Resolution
0.167/mm (at Source and Exit Slit)
Optical Aberration (image tilt)
Δλ/λ < 0.010 at 6 mrad Sagittal Aperture, 10~50 Angstroms (m=1)
Meridonial Aperture
12.5 mrad, on Rowland Circle
Sagittal Aperture
0~30 mrad, astigmatic (Φ)
Exit Slit Width (Vacuum Selectable)
200 µm at 0.2°
100 µm at 0.2° (10-13 Å)
100 µm at 0.7° (13-20 Å)
100 µm at 1.2° (20-28 Å)
100 µm at 1.7° (28-37 Å)
100 µm at 2.2° (> 37 Å)
Exit Slit Length
20 mm
External Drive
Single Micro-Stepped Motor with Compumotor ZETA6104-57-83 Indexer/Drive w/RS232C Interface Port
Vacuum Chamber
Weld-Free 6061 Aluminum, Electroless Nickel Plated; TEFLAT/BLACKFLAT Sealed Knife-edge Ports
Entrance and Exit Ports
4.5″ Conflat Flange (ICF114)
User Ports
Three Ports Accept 2.75″ Conflat Flange (ICF070)
Length
0.63 meters (Slit-Slit)
Aperture Center
Stationary

Construction

Model SNR-SXR-0.6 is a high aperture (Φ = 12.5 mrad), single-element soft x-ray Monochromator. The grating has a 100 mm circular aperture with grooves extending to the edge. The distance from (slitless) source to exit slit is 628 mm. The fixed angular deviation of 4.5 degrees and gold coated grating provide efficient reflection to wavelengths as short as λmin = 10 Angstroms in first order and to approximately 6 Angstroms in second order. The spectral resolution is determined by the sagittal aperture which may be set by knife-edges at the entrance port of exit slit, over the range of approximately 0 to 30 mrad. A typical setting of 3 mrad (illuminating 2 mm at the exit slit) provides a fractional spectral resolution of 1/160 at 23 Å, 1/68 at 50 Å, and 1/33 at 100 Å. However, the long wavelength performance is improved considerably by employing an exit slit mask containing 6 slits (100 µm wide) at different angles, to match the image tilt over different regions in scanned wavelength. Using the appropriate slit, the resolution is approximately 1/100 over 10~50 Å using a 6 mrad sagittal aperture.

An externally mounted micro-stepping motor with Compumotor indexer provides rotational control of the grating scan under vacuum by means of a shaft feedthrough. The slits are also selectable under vacuum using a micrometer shaft feedthrough. Both the grating chamber and the slit chambers are electroless-nickel plated aluminum and are machined square relative to the grating surface and slit mask, enabling alignment by mechanical indication from the chamber exteriors.

The photograph shows a custom system including model SNR-SXR-0.6 and associated optional equipment (not included with base instrument) such as a Manson model 2 soft x-ray source and compact chamber, pumps, gages, mounting table and brackets, CCD, filter assembly, vacuum-selectable aperture and microscope visible alignment system, for calibrating x-ray transmission gratings in the 5-114 Å region.

snr-sxr-fig3

CAL-32

Download product pdf

These anode cap sets are designed to be used with the Manson electron impact sources1, models 2 and 5. As enumerated in the table, the anode library provides a multitude of characteristic lines from K, L and M-shell transitions, as well as Bremsstrahlung continua. The ability to select spectral lines at closely spaced soft x-ray photon energies allows the calibration of spectral features such as filter absorption edges, multilayer (Bragg) interference reflectance peaks and grating efficiency variations (see Fig. 2) without resorting to the use of a synchrotron radiation facility.

The same anode set fits both model 2 and model 5 Manson sources. As specified for each material in the table, the anode caps are constructed of either a) the metal itself, or b) a base of 303 stainless steel with the impact material affixed to the top using low-outgassing silver conductive epoxy. Each anode cap is vented and, following initial break-in, is compatible with vacuum into the 10-8 mbar range. With the exception of Be, all anode caps are reusable indefinitely by nylon pad cleaning of the anode surface after extended use.

Fig. 1 shows the spectrum produced by one typical anode material (zinc), consisting of several useable characteristic L-shell lines, plus an underlying continuum for the atomic number Z=30. As the Bremsstrahlung strength is highly dependent upon Z, the strongest continuum is obtained using tantalum (Z=73) or tungsten (Z=74). Anode set model CAL-32 comprises the following materials: Be(4), B, C, Sapphire, Mg, Al, Si, Sc, Ti, V, Cr, Mn, Fe, SS303, Co, Ni, Cu, Zn, Ge, Y, Zr, Nb, Mo, Ru,Pd, Ag, Sn, Ta and W); refer to the characteristic emission line table for the available photon energies.

As an option, enhanced cooling of the operating anodes is available, using forced-air fans combined with a copper-block finned radiator. This is found to improve the positional stability of the emission region of the Manson source and stabilize its output intensity through reduced hydrocarbon contamination.

cal-32-fig1

Fig. 1. Spectrum of characteristic lines and Bremsstrahlung continuum from a zinc anode in the Manson model 2 source, using Hettrick SXR-II spectrometer and a CCD detector to record the spectrum.

cal-32-fig2
Fig. 2. Absolute efficiency measurements of a free-standing transmission grating, using numerous characteristic lines from CAL-32 anode library and Hettrick SXR-II monochromator.

1 Manson electron impact sources are manufactured and sold by Austin Instruments, Inc.
website: www.austinst.com
email: austinst@tiac.net
tel: 800-818-7403.

Ultimate Posts

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TEFLAT™/BLACKFLAT™ gaskets provide many advantages when compared to conventional sealing materials for knife-edge flanges:

• Require much less force than copper, significantly reducing assembly time (and saving knuckles!).
• May be used with aluminum (or stainless steel) flanges and ports.
• Unlike copper gaskets, Teflon® gaskets are reusable, if not removed from flange and kept clean (number of re-uses may vary).
• Unlike copper gaskets, Teflon® gaskets do not tarnish with exposure to air.
• Unlike copper gaskets or o-rings, Teflon® does not react with most chemicals.
• Avoids the use of grease often necessary to keep thin section o-rings registered in place during assembly, particularly for a vertical flange orientation.
• Minimizes contamination of vacuum systems, particularly important for coating applications, high purity analyses and ultra-high vacuum applications.
• Unlike thin section o-rings, rigid Teflon® gaskets self-locate against the flange lip to provide a clear confirmation of a correct seal, preventing leaks and extruded o-rings.
• Less expensive than rectangular section o-rings.

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